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NMR 1 H (360 MHz, MeOH-d 4 ) : 5.205.05 (m, 5H), 4.72 (d, J = 2.0 Hz, 1H, H-4), 4.24 (dd, J = 11.16 Hz , J = 6.84 Hz, 1H, H-6), 4.18 (dd, J = 11.16 Hz , J = 6.12 Hz, 1H, H-6), 4.08 (ddd, J = 6.84 Hz, J = 6.12 Hz, J = 2.0 Hz, 1H, H-5), 2.46 (t, J = 7.74 Hz, 2H, COC H 2 CH 2 ), 2.30 (t, J = 7.56 Hz, 2H, COCH 2 C H 2 ), 2.121.92 (m, 16H), 1.63 (d, J = 1.08 Hz, 3H, HC = C(C H 3 ) 2 ), 1.62 (s, 3H), 1.60 (s, 12H) ppm

D., Barrett, T., Mitchell, M